Last edited by Taugami
Thursday, May 14, 2020 | History

4 edition of Electron nuclear double resonance spectroscopy of radicals in solution found in the catalog.

Electron nuclear double resonance spectroscopy of radicals in solution

application to organic and biological chemistry

by Harry Kurreck

  • 118 Want to read
  • 8 Currently reading

Published by VCH in New York .
Written in English

    Subjects:
  • Electron nuclear double resonance spectroscopy.,
  • Chemistry, Organic.,
  • Biochemistry.,
  • Radicals (Chemistry)

  • Edition Notes

    StatementHarry Kurreck, Burkhard Kirste, Wolfgang Lubitz.
    SeriesMethods in stereochemical analysis, Methods in stereochemical analysis (Unnumbered)
    ContributionsKirste, Burkhard, 1951-, Lubitz, Wolfgang, 1949-
    Classifications
    LC ClassificationsQD272.S6 K87 1988
    The Physical Object
    Paginationxii, 374 p. :
    Number of Pages374
    ID Numbers
    Open LibraryOL2524961M
    ISBN 100895733242
    LC Control Number88000014

    The flavin adenine dinucleotide (FAD) cofactor of Aspergillus niger glucose oxidase (GO) in its anionic (FAD•-) and neutral (FADH•) radical form was investigated by electron paramagnetic resonance (EPR) at high microwave frequencies ( and GHz) and correspondingly high magnetic fields and by pulsed electron−nuclear double resonance (ENDOR) spectroscopy at Cited by: Double Electron-Electron Resonance Measured Between Gd3+ Ions and Nitroxide Radicals Petra Lueders, Gunnar Jeschke and Maxim Yulikov The Journal of Physical Chemistry Letters, vol. 2: no. 6, pp. , Washington, D.C., USA: American Chemical Society,

      EPR spectra of soluble coffee display single-line free radical signals in both the solid state and aqueous solution, along with signals from the paramagnetic ions Fe(III) and Mn(II). The intensity of the free radical signal in the pure solid was estimated to be ca. x 10(16) unpaired electrons/g, and there was no significant change on Cited by: This is, in part, due to the lack of detailed structural information on the ATPase site in the presence and absence of RNA in solution. We used high-field pulse ENDOR (electron nuclear double resonance) spectroscopy to detect and analyze fine conformational changes in the protein's ATPase site in solution.

    Electron Spin Resonance Spectroscopy Electron Spin Resonance (ESR) spectroscopy, also referred to as Electron Paramagnetic Resonance (EPR) spectroscopy, is a versatile, nondestructive analytical technique based on the absorption of microwave radiation in presence of an applied field by paramagnetic species. Electron paramagnetic resonance (EPR) or electron spin resonance (ESR) spectroscopy is a technique for studying materials with unpaired basic concepts of EPR are analogous to those of nuclear magnetic resonance (NMR), but it is electron spins that are excited instead of the spins of atomic e most stable molecules have all their electrons .


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Electron nuclear double resonance spectroscopy of radicals in solution by Harry Kurreck Download PDF EPUB FB2

The data on electron spin resonance (ESR), electron-nuclear double resonance (ENDOR), and general triple resonance spectroscopy for 2,5-dihydro-1,2,3,5-thiatriazoleyl radicals was reviewed by Holm and Larsen. There are no new data on this subject. This book describes the principles of Endor spectroscopy and Triple resonance, with particular emphasis given to applications in organic chemistry and biochemistry.

It gives a broad survey of Endor studies of organic and bioorganic radicals in solution, but also discusses in detail special topics such as non-proton Endor, multispin systems, dynamic effects, and Endor spectroscopy. Electron nuclear double resonance spectroscopy of radicals in solution.

New York: VCH, © (OCoLC) Online version: Kurreck, Harry, Electron nuclear double resonance spectroscopy of radicals in solution. New York: VCH, © (OCoLC) Document Type: Book: All Authors / Contributors: Harry Kurreck; Burkhard Kirste. ESR, ENDOR, General Triple Resonance NMR Spectroscopy. The data on electron spin resonance (ESR), electron-nuclear double resonance (ENDOR), and general triple resonance spectroscopy for 2,5-dihydro-1,2,3,5-thiatriazoleyl radicals was reviewed by Holm and Larsen.

There are no new data on this subject. Introduction. Electron-nuclear double resonance (ENDOR) has been introduced by Feher in solid state physics and later extended to radicals in solution by Hyde and Maki ().The technique has been extensively used in photosynthesis research (reviewed in Möbius et al.Lubitz and LendzianRigby et al.Britt et al.

).ENDOR combines electron paramagnetic Cited by: TRIPLE Resonance 94 ELDOR 96 6 Taking and Analyzing ESR Spectra 97 Instrumentation 97 g e Factor 99 Optimal Conditions Unravelling Hyperfine Pattern Assignment and Sign of Coupling Constants Ion Pairing Intramolecular Dynamic Processes B Special Part 7 Organic Radicals Centered on.

Electron-nuclear double resonance (ENDOR) has been introduced by Feher in solid state physics and later extended to radicals in solution by Hyde and Maki ().The technique has been extensively used in photosynthesis research (reviewed in Möbius et al.Lubitz and LendzianRigby et al.Britt et al.

).ENDOR combines electron paramagnetic Cited by: H. Kurreck, B. Kirste, W. Lubitz. Electron nuclear double resonance spectroscopy of radicals in solution. Application to organic and biological : L. Sutcliffe. have been described, especially electron-nuclear double resonance (ENDOR) spec-troscopy [12, 15, 16] and its physical fundamentals.

(7) Modern quantum-chemical procedures for calculation of spin distribution in radicals, going beyond the p-electron models, have been briefly presented and their results for particular radicals are quoted.

figures from the ENDOR book (PDF) Electron Nuclear Double Resonance Spectroscopy of Radicals in Solution - Application to Organic and Biological Chemistry - Online Database of EPR and ENDOR Spectra (B.

Kirste, Poster, ). Advanced electron resonance techniques, essentially ENDOR (electron–nuclear double resonance) and pulse EPR, will also be briefly final part of. You can write a book review and share your experiences. Other readers will always be interested in your opinion of the books you've read.

Whether you've loved the book or not, if you give your honest and detailed thoughts then people will find new books that are right for them. Electron nuclear double resonance (ENDOR) spectroscopy of radicals in photosystem I and related Type 1 photosynthetic reaction centres November Biochimica et Biophysica Acta ()   Electron-Nuclear Double Resonance Spectroscopy.

Electron nuclear double resonance (ENDOR) uses magnetic resonance to simplify the electron paramagnetic resonance (EPR) spectra of paramagnetic species (one which contains an unpaired electron).

It is very powerful and advanced and it works by probing the environment of these species. Electron spin resonance spectroscopy is the method used to determine the structure and life expectancy of a number of radicals. Written by Fabian Gerson and Walter Huber, top experts in the field of electron spin resonance spectroscopy, this book offers a compact yet readily comprehensible introduction to the modern world of by: Abstract.

Applications of angle-selected electron nuclear double resonance (ENDOR) spectroscopy using the vanadyl (VO 2+) cation or nitroxyl spin-labels as paramagnetic probes are reviewed in which structured solvent in small molecule and macromolecular complexes have been identified and characterized.

By determination of the principal hyperfine (hf) coupling Cited by: 1. The technique of electron–electron double resonance, in which one part of the EPR spectrum of a paramagnetic sample is irradiated with an intense microwave field and the effect of this intense field on other parts of the spectrum is determined utilizing a second weak microwave field, has been applied to free radicals in solution.

EPR signals detected by the weak microwave source Cited by:   J.A. Pedersen: ‘Handbook of EPR Spectra from Natural and Synthetic Quinones and Quinols’, CRC Press, Boca Raton, FL ().

Kurreck, B. Kirste, W. Lubitz: ‘Electron Nuclear Double Resonance Spectroscopy of Radicals in Solution - Application to Organic and Biological Chemistry’, VCH publishers, Weinheim ().

Identification, by Electron Paramagnetic Resonance Spectroscopy, of Free Radicals Generated from Substrates by Peroxidase* advantage over a double integration in that it is independent nuclear magnetic dipole and the electron dipole.

This term is. Electron paramagnetic resonance (EPR) or electron spin resonance (ESR) spectroscopy is a technique for studying chemical species that have one or more unpaired electrons, such as organic and inorganic free radicals or inorganic complexes possessing a transition metal basic physical concepts of EPR are analogous to those of nuclear magnetic resonance (NMR).

Unlike the photographically important silver halides, large NaCl single crystals can be grown from solution.

In such NaCl crystals, with doping comparable to practical AgCl and AgBr microcrystals, three stable Rh centers were detected and studied by electron paramagnetic resonance (EPR) and electron nuclear double resonance (ENDOR). The primary center was identified as a Cited by: Electron nuclear double resonance spectroscopy -- Congresses.

Electron nuclear double resonance spectroscopy. Electron paramagnetic resonance spectroscopy. Order-disorder models. Ressonancia Magnetica E Relaxacao (Materia Condensada) Modèles ordre-désordre -- Congrès.

Spectroscopie de résonance paramagnétique électronique -- Congrès. The detection of electron magnetic resonance by Zavoiskii in the mid s (1) ushered in a golden age of physical and chemical applications.

Perhaps no single book did more to stimulate this development of EPR spectroscopy than the classic text by Wertz and Bolton (2), which appeared in A revised version, with John A. Weil added as a co-author, was Author: Ffrancon Williams.